A bottom drain cock is desirable but not necessary for removing reagents. This test method requires the use of equipment specifically designed for coulometric titration. No other units of measurement are included in this standard. Plastic syringes shall be disposed of following each sample use. The proposed reaction mechanism is as follows:
|Date Added:||22 April 2013|
|File Size:||40.27 Mb|
|Operating Systems:||Windows NT/2000/XP/2003/2003/7/8/10 MacOS 10/X|
|Price:||Free* [*Free Regsitration Required]|
The degree of saturation of the water-saturated 1-Octanol varies. Current edition approved Dec. It may consist of two platinum meshes or wires separated by a diaphragm within a glass assembly astm d1533 two platinum meshes or wires not astm d1533 by a diaphragm. It is the responsibility of the user of this standard to establish appropriate safety and health practice and determine the applicability of regulatory limitations prior to use. The ast specimen is injected into a titration cell where the iodine consumed by the axtm with water is electrolytically regenerated by anodic oxidation of iodide.
Refer to Annex A1 for information on alternative solvent systems. Originally approved in Summary of Test Method 3. Stirring should be at such a rate that an oil layer will not form on top of the reagent. astm d1533
No further reproductions authorized. If this drifting end point cannot be corrected, the water values should be regarded as suspect. Size px x astm d1533 x x Remove the sample aliquot from the top phase and inject aztm immediately into the titration cell. In a sealed system, recleaning and redrying are not necessary for routine use. They should be of a large enough gauge to allow for easy transfer of astm d1533 sample.
Significance and Use 4. Karl Fischer instruments regenerate iodine coulometrically from the iodide in the Karl Fischer asttm.
If a drifting end point is noted, an alternative solvent system or another titration method is warranted. We are a non-profit group that run this astm d1533 to share documents. Astmm other units of measurement are included in this standard. The proposed reaction mechanism is as follows: Wiley and Sons, Inc. We need your help to maintenance this website.
Astm d – Free Download PDF
NOTE 1—For the best accuracy the solution should not be mixed or shaken after standing. This test method requires the use of equipment specifically designed for coulometric titration. A bottom drain cock is desirable but not necessary for removing reagents. This standard has been approved for use by agencies of the Department of Defense.
In the cell with a diaphragm the cathode astm d1533 contains similar reagents optimized for cathodic reduction. Syringes may be glass or plastic. If accurate results can not be obtained, the solution should be discarded.
Please fill this form, we will try astm d1533 respond as soon as possible. A high water 4 Scholz, E. Last previous edition approved in as D — 00 We need your help! Thank you for interesting in our services. Excess oil may not mix thoroughly with the solvent system thus preventing the total water content of that test specimen from being measured properly. astm d1533